HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19806576, compound → HCID 19806593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19806576 | HCID 19806576 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 19806593 | HCID 19806593 | 100% |
Reaction Steps
A mixture of 5-(2-methylimidazol-1-yl)-2-nitrobenzylalcohol (308 mg), 10% Pd/C(84 mg) and methanol (5.0 ml) was hydrogenated at 1 atmosphere. The mixture was stirred at room temperature for 2 hours and filtered to remove the catalyst. The filtrate was diltilled under reduced pressure to give 268 mg (100%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171851 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-7c3c9ab6955744e8ae1ca2d7653bb27f |
| Source note | uspto-grants-1992_12 |