HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14450253, compound → HCID 14450266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14450253 | HCID 14450253 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14450266 | HCID 14450266 | 87.6% |
Reaction Steps
A mixture of 5-(4-methylimidazol-1-yl)-2-nitrotoluene (198 mg), 10% Pd/C (58 mg) and methanol (3.0 ml) was hydrogenated with hydrogen of 1 atmosphere. The mixture was stirred at room temperature for 2 hours and filtered. The filtrate was distilled under reduce pressure to give 149 mg (87.6%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171851 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-8250fed234b04db287ab4bd857b24f78 |
| Source note | uspto-grants-1992_12 |