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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1681388Generated: November 4, 2026

HCID 14450253, compound → HCID 14450266, compound

https://huagongshe.com/reaction/1681388

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 14450253HCID 14450253—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 14450266HCID 1445026687.6%

Reaction Steps

A mixture of 5-(4-methylimidazol-1-yl)-2-nitrotoluene (198 mg), 10% Pd/C (58 mg) and methanol (3.0 ml) was hydrogenated with hydrogen of 1 atmosphere. The mixture was stirred at room temperature for 2 hours and filtered. The filtrate was distilled under reduce pressure to give 149 mg (87.6%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05171851
Source datasetuspto-grants-1992_12
ORD IDord-8250fed234b04db287ab4bd857b24f78
Source noteuspto-grants-1992_12