Iodine chloride → HCID 19806575, compound

Participants

Reaction Steps

A mixture of 2-amino-5-(4-methylimidazol-1-yl)toluene (100 mg), iodomono-chloride (104 mg) and acetic acid (1.3 ml) was stirred at room temperature for 2 hours. Solvent was removed under reduced pressure to give a residue. The residue was made to pH 10 with saturated sodium bicarbonate solution, extracted with chloroform. The extract was dried with MgSO4, filtered and removed solvent to give 68 mg (41%) of the title compound.

Provenance & Evidence