Methanol → HCID 67918065, compound

Participants

Reaction Steps

2-amino-3-methyl-5-(4-methylimidazol-1-yl)benzaldehyde (57 mg) was dissolved in methanol (1 ml) and sodiumborohydride (40 mg) was added thereto at 0° C. The mixture was stirred at room temperature for 6 hours and was distilled under reduced pressure to remove solvent. To the residue was added water. The mixture was extracted with chloroform. The extract was dried with Na2SO4 and distilled to give 34 mg (59%) of the title compound.

Provenance & Evidence