HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13764026, compound → HCID 13764034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13764026 | HCID 13764026 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13764034 | HCID 13764034 | — |
Reaction Steps
Combine 15 g (59 mmol) of the product of Example IV with 150 g of manganese dioxide in 500 ml of methylene chloride and heat at reflux for 24 hr. Filter off the solids and remove the solvents under vacuum. Crystallize the residue from ethyl acetate to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171858 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-a54e52d530d044ba9c45640b3ba5f9be |
| Source note | uspto-grants-1992_12 |