HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylimidazole → HCID 13764013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylimidazole | HCID 12749 | — |
| Reactant | 4-Chlorobutyrophenone | HCID 253533 | — |
| Product | HCID 13764013 | HCID 13764013 | — |
Reaction Steps
Combine 270 g (1.48 mol) of 4-chlorobutyrophenone with 600 g (7.3 mol) of 2-methylimidazole and heat to 175° C. for 24 hr. Crystallization from ether provides the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171858 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-00e44750469b430c94d5050e11e7fb4c |
| Source note | uspto-grants-1992_12 |