HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenethylamine, (+)- → HCID 15671289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenethylamine, (+)- | HCID 643189 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | Methyl 6-fluoro-4-oxo-4H-1-benzopyran-2-carboxylate | HCID 14089205 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 15671289 | HCID 15671289 | — |
Reaction Steps
Sodium methoxide (540 mg, 10.0 mmol) was added to a solution of methyl 6-fluoro-4-oxo-4H-1-benzopyran-2-carboxylate (2.22 g, 10.0 mmol, obtained in Example 3 or 4) and (R)-α-methylbenzylamine (1.21 g, 10.0 mmol) in dry benzene (20 ml) and the mixture was refluxed for 2 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171865 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-db76c8ce8a704c1e837b9e091bf86f90 |
| Source note | uspto-grants-1992_12 |