HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenemethanesulfonamide → Methyl oxo[(phenylmethanesulfonyl)amino]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenemethanesulfonamide | HCID 78318 | — |
| Reactant | Methyl chloroglyoxylate | HCID 79846 | — |
| Product | Methyl oxo[(phenylmethanesulfonyl)amino]acetate | HCID 13186355 | — |
Reaction Steps
A mixture of benzylsulfonamide (16.7 g, 0.0975 mole) and methyloxalylchloride (38 ml, 0.41 mol) was heated at 100°-120° C. for 2 hours. Upon evaporation, there was obtained the title compound, 20.6 g, mp 119°-124° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05171860 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-90eb4b80eff44321871539d18c42fae0 |
| Source note | uspto-grants-1992_12 |