HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 19762694, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 18371174 | HCID 18371174 | — |
| Product | HCID 19762694 | HCID 19762694 | 100% |
Reaction Steps
1.24 g (5 mmoles) of 3-(1-methylcyclohexyl)-4-methoxybenzoic acid and 15 ml of thionyl chloride are heated at reflux until the cessation of gas evolution. The reaction mixture is evaporated to dryness. 1.32 g (100% yield) of crude 3-(1-methylcyclohexyl)-4-methoxybenzoic acid chloride which is used as such for the following synthesis are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05173289 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-4e7f54a7c9e3402b923644cda1740b25 |
| Source note | uspto-grants-1992_12 |