HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19805341, compound → HCID 19805333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19805341 | HCID 19805341 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19805333 | HCID 19805333 | — |
Reaction Steps
12 g (37.4 mmol) 1-benzyl-3-(tert.butoxy-carbonylamino-methyl)-3-methoxymethylpyrrolidine is desolved in 150 ml ethanol. This solution is hydrogenated at 4 g Pd-carbon (10%) at 100° C./100 bar H2. The catalyst is removed by filtration, and the organic solvents are removed in vacuo. The residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05173484 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-ea7059bf16bc489e97e62378663e87b5 |
| Source note | uspto-grants-1992_12 |