HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethoxypropane → HCID 178450587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethoxypropane | HCID 6495 | — |
| Reactant | Pantethine | HCID 452306 | — |
| Catalyst | Trifluoroacetic acid | HCID 6422 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178450587 | HCID 178450587 | — |
Reaction Steps
A mixture of 1.0 g of D-pantethine, 5 ml of 2,2-dimethoxypropane, 5 drops of trifluoroacetic acid and 5 ml of acetone was stirred for 2 days and then evaporated. The resulting white foam was purified by flash chromatography [dichloromethane:methanol (10:1)], giving 1.0 g of the desired compound as a white hygroscopic foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05173510 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-026ceb9ae02f4d6caab782b05ebeefc8 |
| Source note | uspto-grants-1992_12 |