HRID1681683

反应详情

EQUATION

反应方程式

HRID 1681683 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Preparation of titanium trichloride composition-n-Hexane (6 l), diethylaluminum monochloride (DEAC) (5.0 mols) and diisoamyl ether (12.0 mols) were mixed at 25° C. for 5 minutes, followed by reacting the mixture at the same temperature, for 15 minutes to obtain a reaction solution (I) (the molar ratio of diisoamyl ether/DEAC: 2.4).

WORKUP

后处理

  1. additionwere mixed at 25° C. for 5 minutes