HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopentyl ether → diisoamyl ether DEAC
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopentyl ether | HCID 10989 | — |
| Reactant | Diethyl aluminum chloride | HCID 16686102 | — |
| Catalyst | titanium(III) trichloride | HCID 10313229 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | diisoamyl ether DEAC | HCID 131713250 | — |
Reaction Steps
Preparation of titanium trichloride composition-n-Hexane (6 l), diethylaluminum monochloride (DEAC) (5.0 mols) and diisoamyl ether (12.0 mols) were mixed at 25° C. for 5 minutes, followed by reacting the mixture at the same temperature, for 15 minutes to obtain a reaction solution (I) (the molar ratio of diisoamyl ether/DEAC: 2.4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05173540 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-2afcdbcb04a0490fad9c60a07db7fe7c |
| Source note | uspto-grants-1992_12 |