HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1682021Generated: October 29, 2026
HCID 13292504, compound → HCID 14306844, compound
https://huagongshe.com/reaction/1682021
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 13292504 | HCID 13292504 | — |
| Reactant | (Pyrrolidin-3-yl)methanol | HCID 13400657 | — |
| Product | HCID 14306844 | HCID 14306844 | — |
Reaction Steps
A mixture of 3.6 g (29.4 mmol) of 3-hydroxymethyl-pyrrolidine and 4.7 g (14.7 mmol) of 2-(2-bromoethyl)-6-methoxy-naphthalene is heated to 120° C. for 2 hours. The reaction mixture is purified over 200 g of silica gel (0.063-0.2 mm) with methylene chloride and then with increasing amounts of ethanol (up to 5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05175157 |
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| Source dataset | uspto-grants-1992_12 |
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| ORD ID | ord-e5d44a641f6a4a039ad2b5d69bd939fb |
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| Source note | uspto-grants-1992_12 |
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