HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14306769, compound → HCID 14306777, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14306769 | HCID 14306769 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14306777 | HCID 14306777 | — |
Reaction Steps
Prepared from 3-[(N-(2-(6,7-dimethoxy-isoquinol-4-yl)-ethyl)-piperidin-3-yl)-methyl]-7,8-dimethoxy-2-oxo-1,3-dihydro-2H-3benzazepine by hydrogenation at 5 bar hydrogen pressure with 10% palladium/charcoal in ethanol at 70° C. analogously to Example 5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05175157 |
| Source dataset | uspto-grants-1992_12 |
| ORD ID | ord-ec2216a7d2b44be8864258b11b7246fe |
| Source note | uspto-grants-1992_12 |