Ammonium formate → HCID 67689997, compound

Participants

Reaction Steps

A mixture of 2-amino-6-Chloro-9-[1-(2,2-dimethyl-1,3-dioxane-4,6-dione-5-yl)eth-2-yl]purine potassium salt (200 mg, 0.53 mmol), ammonium formate (148 mg, 2.34 mmol) and 10% palladuim on charcoal (80 mg) in methanol (15 ml) was heated under reflux under dry nitrogen for 3 h. T.1.c. [chloroform/methanol (2:1)] showed one spot, rf=0.15. The mixture was filtered and the filtrate evaporated to leave a gum. The material was not purified further.

Provenance & Evidence