3-Amino-1-propanol → N-Benzoyl-4-oxacaprolactam

HRID 1682377Notes

Reaction equation

HRID 1682377 reaction equation
[C:1]([N:9]1[CH2:14][CH2:13][O:12][CH2:11][C:10]1=[O:15])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.N[CH2:17]CCO>>[C:1]([N:9]1[CH2:14][CH2:13][O:12][CH2:11][CH2:17][C:10]1=[O:15])(=[O:8])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 90863-Amino-1-propanolHCID 122940964-Benzoylmorpholin-3-one

Product 1

HCID 19043817N-Benzoyl-4-oxacaprolactam

Procedure

Synthesized as for N-benzoyl-3-oxomorpholine (Example I) using 3-aminopropanol (Aldrich) in place of 2-aminoethanol.

Sources & evidence

ORD record
ord-72d3c5bb9f5f476e919890e634962cb7
Source dataset
uspto-grants-1997_06
Patent number
US05635103

Reaction notes

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