HuagongsheHuagongshe Chemistry Print Report · For research reference only
Palladium Chloride → Palladium triflate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Palladium Chloride | HCID 24290 | — |
| Reactant | Trifluoromethanesulfonic acid | HCID 62406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Palladium triflate | HCID 11603820 | — |
Reaction Steps
PdCl2 (1.0 g, 5.6 mmol) was slurried in CH2Cl2 (20 mL) and triflic acid (1.7 g, 11.3 mmol) was added dropwise. The mixture was stirred at room temperature overnight. The solvent was removed and 0.9 g of rust color solid was collected. 19F NMR (CDCl3): δ-5 78.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05635585 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-f53ff08b482544a3899a442bed6f5ef3 |
| Source note | uspto-grants-1997_06 |