HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 167263-05-0
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | Tert-butyl 4-cyano-4-(pyridin-2-YL)piperidine-1-carboxylate | HCID 53439111 | — |
| Product | 167263-05-0 | HCID 67322272 | — |
Reaction Steps
Prepare by the method of example 30.3 using 1-tert-butoxycarbonyl-4-cyano-4-(pyridin-2-yl)-piperidine (3 mmol) and HCl in dioxane (40 mmol, 4N). Concentrate the solvent in vacuo and dry under high vacuum to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05635510 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-ff7271a5c2654dbe9c2463f023de724e |
| Source note | uspto-grants-1997_06 |