HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(3-(3,4-Dichlorophenyl)pyrrolidin-3-yl)ethanol → 2-[3-(3,4-Dichloro-phenyl)-1-(3-isopropoxy-phenacyl)-pyrrolidin-3-yl]-ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(3-(3,4-Dichlorophenyl)pyrrolidin-3-yl)ethanol | HCID 18464427 | — |
| Reactant | 2-Chloro-1-[3-(1-methylethoxy)phenyl]ethanone | HCID 54076023 | — |
| Product | 2-[3-(3,4-Dichloro-phenyl)-1-(3-isopropoxy-phenacyl)-pyrrolidin-3-yl]-ethanol | HCID 54141067 | — |
Reaction Steps
Prepare by the method of example 3.1 using 2-[3-(3,4-dichloro-phenyl)-pyrrolidin-3-yl]-ethanol (2 mmol) and 3-isopropoxy-phenacyl chloride (2 mmol). Chromatograph on silica gel to give the title compound. Rf =0.44 (silica gel, 5% methanol/dichloromethane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05635510 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-134b0c25d58a4b0381de52e7aef41709 |
| Source note | uspto-grants-1997_06 |