Triethylamine → HCID 178420583, compound

HRID 1683301Notes

Reaction equation

HRID 1683301 reaction equation
[Cl-:1].[Cl-].[Cl-].[CH:4]1([Ti+3:9])[CH:8]=[CH:7][CH:6]=[CH:5]1.[OH:10][C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][N:12]=1.C(N(CC)CC)C>CCOCC>[Cl-:1].[Cl-:1].[CH:4]1([Ti+2:9][O:10][C:11]2[CH:16]=[CH:15][CH:14]=[CH:13][N:12]=2)[CH:8]=[CH:7][CH:6]=[CH:5]1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 178478623HCID 178478623, compoundHCID 178516071HCID 178516071, compound

Product 1

HCID 178420583HCID 178420583, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent2×

Procedure

To a solution of 0.002 moles of cyclopentadienyl titanium trichloride in 50 mL of ether a solution of 2-hydroxy pyridine (0.002 moles) and triethylamine (0.002 moles) in 50 mL of ether was added at 0° C. and stirred overnight. The product was recovered from the ether filtrate. The product has the formula: ##STR12##

Workup

  1. customThe product was recovered from the ether filtrate

Sources & evidence

ORD record
ord-0800c60309ea4b45aa7e55e7242a29dd
Source dataset
uspto-grants-1997_06
Patent number
US05637660

Reaction notes

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