HRID1683304

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID22999080

2,3-Dimethoxy-3-oxopropanoate

C5H7O5-

结构：CC(C)(C)OC(=O)NC(=NCCCCCCCCN)NC(=O)OC(C)(C)C

HCID25214054

未命名化合物

PRODUCTS

生成物

结构：COC(=O)C(OC)C(=O)NCCCCCCCCNC(=NC(=O)OC(C)(C)C)NC(=O)OC(C)(C)C

HCID178501832

未命名化合物

收率 95%

PROCEDURE

实验过程

By following a procedure analogous to the method of Preparation 18, using 3.5 g (23.65.10-3 mol) of methyl 2-methoxypropanedioate and 7 g (18.1.10-3 mol) of bis(1,1-dimethylethyl) [[(8-aminooctyl)imino]methylene]biscarbamate as the starting materials, 8.6 g (yield=95%) of the expected product are obtained in the form of a yellow oil.

WORKUP

后处理

customto the method of Preparation 18