HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-Dimethoxy-3-oxopropanoate → HCID 178501832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-Dimethoxy-3-oxopropanoate | HCID 22999080 | — |
| Reactant | Bis(1,1-dimethylethyl) [[(8-aminooctyl)imino]methylene]biscarbamate | HCID 25214054 | — |
| Product | HCID 178501832 | HCID 178501832 | 95% |
Reaction Steps
By following a procedure analogous to the method of Preparation 18, using 3.5 g (23.65.10-3 mol) of methyl 2-methoxypropanedioate and 7 g (18.1.10-3 mol) of bis(1,1-dimethylethyl) [[(8-aminooctyl)imino]methylene]biscarbamate as the starting materials, 8.6 g (yield=95%) of the expected product are obtained in the form of a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05637613 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-52ee23ce7f68449cba206de89f0aeb7e |
| Source note | uspto-grants-1997_06 |