Hydrogen Bromide → HCID 86750952, compound

Participants

Reaction Steps

In a manner similar to that described above, 3,3-bis(heptafluorobutoxymethyl)oxetane (250.0 g, 0.52 mole) was reacted with 48% HBr (131.7 g, 0.78 mole) to give 260.9 g (89.1%) of 3-bromo-2,2-bis(heptafluorobutoxymethyl)-1-propanol, a clear oil: 1H NMR (CDCl3) 3.49 (s, 2H), 3.65 (s, 4H), 3.69 (s, 2H), and 3.95 (t, J=13.3 Hz, 2H); Anal. Calcd for C13H13BrF14O3 : C, 27.72; H, 2.33; Br, 14.19; Found: C, 27.73; H, 2.27; Br, 14.09.

Provenance & Evidence