HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromopinacolone → HCID 2851567, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromopinacolone | HCID 21642 | — |
| Reactant | 2-((1H-1,3-benzodiazol-2-yl)amino)ethan-1-ol | HCID 583867 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Product | HCID 2851567 | HCID 2851567 | — |
Reaction Steps
Heat at reflux for 3 hours a mixture of 2-(2-hydroxyethylamino)benzimidazole (1.77 g, 10 mmol) and bromopinacoline (1.35 g, 10 mmol) in 50 ml of propanol. Subsequently maintain at room temperature. The next day, the title compound is collected by filtration and washed with acetone and then with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05639756 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-ab2d8f01f98348bd9b410527648cab5a |
| Source note | uspto-grants-1997_06 |