Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Bromine | HCID 24408 | — |
| Reactant | HCID 15541469 | HCID 15541469 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 18511696 | HCID 18511696 | — |
Reaction Steps
0.19 ml of bromine was dropwise added to a solution of 0.88 g of 2-ethoxycarbonyl-3-acetyloxy-6-acetylpyridine dissolved in 8.8 ml of acetic acid. The mixture was stirred at 75° C. for 5 minutes to obtain 0.77 g of 2-ethoxycarbonyl-3-hydroxy-6-(2-bromoacetyl)pyridine hydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05639770 |
|---|
| Source dataset | uspto-grants-1997_06 |
|---|
| ORD ID | ord-c16193f2917f481a83baa183af809a4c |
|---|
| Source note | uspto-grants-1997_06 |
|---|
