HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phthalic Anhydride → HCID 16789391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | 4-Aminophenylacetic acid | HCID 14533 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 16789391 | HCID 16789391 | — |
Reaction Steps
Phthalic acid anhydride (15.1 g, 102 mmol) and 4-amino phenyl acetic acid (15.2 g, 102 mmol) were dissolved in acetic acid and heated at reflux for 1 hour. Upon cooling on an ice bath, the product crystallized. The solid was filtered off, washed with water, and dried under vacuum overnight. The yield of the title compound was 24.1 g (86%) as an off white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05639778 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-fce27708133e44edb114726a1657e116 |
| Source note | uspto-grants-1997_06 |