HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 45050441, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Dimethyl Succinate | HCID 7820 | — |
| Product | HCID 45050441 | HCID 45050441 | 4.9% |
Reaction Steps
Benzaldehyde (21.2 g) and succinic acid dimethyl ester (40.9 g) are treated in the same manner as in Reference Example 1, and the resulting product is purified by silica gel column chromatography to give (Z)-3-methoxycarbonyl-4-phenyl-3-butenoic acid methyl ester (2.3 g) as colorless syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05639789 |
| Source dataset | uspto-grants-1997_06 |
| ORD ID | ord-0744193b23f94874828e643f521368ff |
| Source note | uspto-grants-1997_06 |