Potassium Carbonate → HCID 19039064, compound

Participants

Reaction Steps

8.3 g (60 mmols) of potassium carbonate was added to a mixture of 6.8 g (20 mmols) of 4-bromomethyl-1-n-pentyl-1-phenyl-1-silacyclohexane, 3.6 g (20 mmols) of 4-trifluoromethoxyphenol and 50 ml of dimethylformamide (DMF), followed by heating under flux for 10 hours. The reaction mixture was after-treated by a usual manner and purified through chromatography to obtain 6.4 g (yield: 73%) of 4-(4-trifluoromethoxyphenyloxymethyl)-1-n-pentyl-1-phenyl-1-silacyclohexane. The results of IR and NMR analyses are shown below.

Provenance & Evidence