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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1684513Generated: October 29, 2026

11-(Chloroacetyl)-5,11-dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-one → HCID 19039393, compound

https://huagongshe.com/reaction/1684513

Reaction equation

Participants

RoleNameHCIDCharge
Reactant11-(Chloroacetyl)-5,11-dihydro-6H-pyrido(2,3-b)(1,4)benzodiazepin-6-oneHCID 120053—
ReactantHCID 19039423HCID 19039423—
ProductHCID 19039393HCID 19039393—

Reaction Steps

Prepared analogously to Example 8 from 11-(chloroacetyl)-5,11-dihydro-6H-pyrido[2,3-b][1,4]-benzodiazepin-6-one and 3-[3-[(acetyl)methylamino]-propyl]piperidine. Purification is carried out by chromatography on silica gel (Baker) using methylene chloride to which increasing amounts of methanol are added.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05641772
Source datasetuspto-grants-1997_06
ORD IDord-6d99d7b7eebf48659965092c76dcf594
Source noteuspto-grants-1997_06