Diethylamine → 2-(N,N-diethylaminomethyl)-4-(3,4-dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxyquinoline

Participants

Role	Name	HCID	Charge
Reactant	Diethylamine	HCID 8021	—
Reactant	2-Bromomethyl-4-(3,4-dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxyquinoline	HCID 19039898	—
Product	2-(N,N-diethylaminomethyl)-4-(3,4-dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxyquinoline	HCID 54418339	—

Reaction Steps

According to the same manner as that described in Example 1, 2-bromomethyl-4-(3,4-dimethoxyphenyl)-6,7-dimethoxy-3-hexanoylquinoline was reacted with diethylamine to give 2-(N,N-diethylaminomethyl)-4-(3,4-dimethoxyphenyl)-3-hexanoyl-6,7-dimethoxyquinoline. This compound was recrystallized from ethyl acetate - hexane to give colorless prisms. mp. 104°-106° C.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US05641788
Source dataset	uspto-grants-1997_06
ORD ID	ord-1938e9e4417a48f69cf37b2d334517fe
Source note	uspto-grants-1997_06