huagongshe.com
HRID1684888

反应详情

EQUATION

反应方程式

HRID 1684888 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CCOC(=O)[C@H](C)N.Cl
HCID2724356

(S)-Ethyl 2-aminopropanoate hydrochloride

C5H12ClNO2

结构：O=P(Cl)(Cl)OP(=O)([O-])Oc1ccc(Cl)cc1
HCID86761540

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)[C@H](C)NP(=O)(Cl)Oc1ccc(Cl)cc1
HCID44226153

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Following the procedure described for Step 1 of Example 1, treatment of a DCM (0.16 M) solution of para-chlorophenyl dichlorodiphosphate with L-alanine ethyl ester hydrochloride (1.0 eq.) and Et3N (2.0 eq.) provided the title compound as a colourless oil as a 1:1 mixture of diastereomers.