HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 86661276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | HCID 58055059 | HCID 58055059 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86661276 | HCID 86661276 | — |
Reaction Steps
The 1-(3,4-dichloro-benzyl)-3-(4-iodomethyl-thiazol-2-yl)-urea (Intermediate 6, 0.3 mmol) was taken up in a 2.0 M solution of ethylamine in tetrahydrofuran (5 ml). Reaction was stirred at room temperature for 1 hour. The volatiles were removed in vacuo and the crude title compound was taken on as is, ˜75% pure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148380B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ffb93c545aa84d1abd32b0be5882851d |
| Source note | uspto-grants-2012_04 |