HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-isocyanatoethyl)thiophene → HCID 86628145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-isocyanatoethyl)thiophene | HCID 2782179 | — |
| Reactant | HCID 178426134 | HCID 178426134 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86628145 | HCID 86628145 | — |
Reaction Steps
In analogy to example 1c, 200 mg (1.09 mmol) of 6-chloro-4-methyl-1H-pyrazolo-[3,4-b]pyridin-3-ol were reacted with 183.5 mg (1.19 mmol) of 2-(2-isocyanatoethyl)-thiophene in THF at room temperature. Yield: 184 mg (50%), M+H+: 337.09.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148395B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-192098d6eda9461c8b44eb443bf8a18e |
| Source note | uspto-grants-2012_04 |