HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isocyanato-1,2,3,4-tetrahydronaphthalene → HCID 86628150, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isocyanato-1,2,3,4-tetrahydronaphthalene | HCID 16217239 | — |
| Reactant | HCID 178426134 | HCID 178426134 | — |
| Solvent | tetrahydrofuran N,N-dimethylformamide | HCID 21974620 | — |
| Product | HCID 86628150 | HCID 86628150 | — |
Reaction Steps
In analogy to example 1c, 200 mg (1.089 mmol) of 6-chloro-4-methyl-1H-pyrazolo-[3,4-b]pyridin-3-ol were reacted with 226.4 mg (1.2 mmol) of 1-isocyanato-1,2,3,4-tetrahydronaphthalene in THF/DMF at RT. Yield: 142 mg (37%), M+H+: 357.35.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148395B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-191789458c5c4d58af815c4aed596ba6 |
| Source note | uspto-grants-2012_04 |