HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Azaindole → 3-(1,2,3,5,8,8a-Hexahydro-7-indolizinyl)-1H-6-azaindole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Azaindole | HCID 9219 | — |
| Reactant | Pyrrolidine | HCID 31268 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3-(1,2,3,5,8,8a-Hexahydro-7-indolizinyl)-1H-6-azaindole | HCID 9881227 | — |
Reaction Steps
from 6-azaindole (250 mg, 2.1 mmol), 1,2,3,5,6,8,8a-heptahydrohydro-7-oxo-indolizine (324 mg, 2.3 mmol) and pyrrolidine (1.2 g, 16.9 mmol) in ethanol (2 mL) heating at reflux for 6 hrs.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148394B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-e33c7ee25f53437ebf248e1d1d29d06d |
| Source note | uspto-grants-2012_04 |