HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Cyanobenzyl alcohol → HCID 178513316, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Cyanobenzyl alcohol | HCID 160549 | — |
| Reactant | HCID 178426655 | HCID 178426655 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 178513316 | HCID 178513316 | — |
Reaction Steps
The title compound is prepared in analogy to rac-4-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-N-hydroxy-3,5-dimethyl-benzamidine (step b) starting from 4-hydroxymethyl-benzonitrile and using triethylamine as base; LC-MS: tR=0.21 min, [M+1]+=167.04.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148410B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-c2a9cbc941bb4be896b4552ec594e448 |
| Source note | uspto-grants-2012_04 |