HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Amino-3-chloro-5-methylbenzonitrile → HCID 178426663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Amino-3-chloro-5-methylbenzonitrile | HCID 2735301 | — |
| Reactant | HCID 178426654 | HCID 178426654 | — |
| Product | HCID 178426663 | HCID 178426663 | — |
Reaction Steps
The title compound is prepared from commercially available 4-amino-3-chloro-5-methylbenzonitrile in analogy to 4,N-dihydroxy-3,5-dimethyl-benzamidine; LC-MS: tR=0.50 min; [M+1]+=200.01; 1H NMR (D6-DMSO): δ 2.15 (s, 3H), 5.20 (s, 2H), 5.61 (s, 2H), 7.28 (s, 1H), 7.40 (s, 1H), 9.33 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148410B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-5dbcf2d75328445abdb8d91caf9f25f1 |
| Source note | uspto-grants-2012_04 |