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HRID1685735

反应详情

EQUATION

反应方程式

HRID 1685735 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1ccc(C(=O)O)s1
HCID818882

5-Formyl-2-thiophenecarboxylic Acid

C6H4O3S

结构：Cc1cc(C(=N)NO)cc(C)c1O
HCID178426654

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(-c2noc(-c3ccc(C=O)s3)n2)cc(C)c1O
HCID136377325

未命名化合物

收率 15.5%

PROCEDURE

实验过程

The title compound (140 mg) is prepared from 5-formyl-2-thiophene carboxylic acid (468 mg, 3.0 mmol) and 4,N-dihydroxy-3,5-dimethyl-benzamidine (540 mg, 3.0 mmol) according to Method A; LC-MS: tR=1.01 min; [M+1]+=301.04; 1H NMR (D6-DMSO): δ2.24 (s, 6H), 7.64 (s, 2H), 8.17 (s, 2H), 8.99 (s, 1H), 10.06 (s, 1H).