HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57700027, compound → HCID 136000909, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57700027 | HCID 57700027 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Solvent | Thioanisole | HCID 7520 | — |
| Product | HCID 136000909 | HCID 136000909 | — |
Reaction Steps
A mixture of N-[4-(7-benzyloxy-3-bromo-6-methoxy-quinolin-4-yloxy)-phenyl]-benzamide (35 mg, 0.063 mmol) in TFA (1 ml) and thioanisole (80 μl) was refluxed for 4 hours, cooled and concentrated under high vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148531B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-b1be0ab8632f4f40bd77c82596c713c8 |
| Source note | uspto-grants-2012_04 |