HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67264705, compound → HCID 136387228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67264705 | HCID 67264705 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Solvent | Thioanisole | HCID 7520 | — |
| Product | HCID 136387228 | HCID 136387228 | — |
Reaction Steps
A mixture of N-[4-(7-benzyloxy-3-cyclopropyl-6-methoxy-quinolin-4-yloxy)-phenyl]-benzamide (50 mg, 0.097 mmol) in TFA (750 μl) and thioanisole (90 μl) was refluxed for 1 hour, cooled and concentrated under high vacuum to use crude in the next stage.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148531B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-5e80a447825e4c639ff3218cf2119b5e |
| Source note | uspto-grants-2012_04 |