HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66686258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 11708802 | HCID 11708802 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 66686258 | HCID 66686258 | 82.5% |
Reaction Steps
2,3-dimethyl-4-(4-fluorobenzylamino)-1H-pyrrolo[3,2-c]pyridine (1.44 g, 5.34 mmol) prepared in Example 32 was dissolved in ethyl acetate (10 ml). The reaction mixture was saturated with hydrochloric acid gas and then filtered to give the titled compound as a white solid. (Yield: 82.5%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148529B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-6423cfd6a44b42feb7cd6fdf6fd1a81e |
| Source note | uspto-grants-2012_04 |