Methanesulfonyl chloride → HCID 86643789, compound

HRID 1686134Notes

Reaction equation

HRID 1686134 reaction equation
[CH3:1][S:2](Cl)(=[O:4])=[O:3].[CH:6]1([CH2:12][CH2:13][CH:14]([OH:16])[CH3:15])[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1>C(Cl)Cl>[CH3:1][S:2]([O:16][CH:14]([CH3:15])[CH2:13][CH2:12][CH:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1)(=[O:4])=[O:3]

Participants

4

Reactant 2

HCID 31297Methanesulfonyl chlorideHCID 112065alpha-Methylcyclohexanepropanol

Product 1

HCID 86643789HCID 86643789, compoundYield 107.5%

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent2×

Procedure

A solution of 3.53 g methanesulfonyl chloride in 100 mL methylene chloride was added to a solution of 4.38 g 4-cyclohexylbutan-2-ol in 200 mL methylene chloride. The reaction mixture was stirred over night. Aqueous work-up yielded 7.06 g (96%) of a colourless oil.

Sources & evidence

ORD record
ord-380e1845775c4597bf39768a151e6233
Source dataset
uspto-grants-2012_04
Patent number
US08148538B2

Reaction notes

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