HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 86643789, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | alpha-Methylcyclohexanepropanol | HCID 112065 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86643789 | HCID 86643789 | 107.5% |
Reaction Steps
A solution of 3.53 g methanesulfonyl chloride in 100 mL methylene chloride was added to a solution of 4.38 g 4-cyclohexylbutan-2-ol in 200 mL methylene chloride. The reaction mixture was stirred over night. Aqueous work-up yielded 7.06 g (96%) of a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148538B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-380e1845775c4597bf39768a151e6233 |
| Source note | uspto-grants-2012_04 |