Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Phthalimide | HCID 6809 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 86643789 | HCID 86643789 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67264543 | HCID 67264543 | 58.1% |
Reaction Steps
A solution of 7.00 g 3-cyclohexyl-1-methylpropyl methanesulfonate in 20 mL DMF was added to a solution of 5.14 g phthalimide and 7.43 g of potassium carbonate in 50 mL DMF at room temperature. The reaction mixture was stirred at 80° C. over night. Aqueous work-up followed by silica gel filtration yielded 4.95 g (58%) of a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08148538B2 |
|---|
| Source dataset | uspto-grants-2012_04 |
|---|
| ORD ID | ord-9b15a064074541ae9b5f2ac89c013c7c |
|---|
| Source note | uspto-grants-2012_04 |
|---|
