HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → Cyclohexanepropanamine, alpha-methyl- (9CI)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 67264543 | HCID 67264543 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Cyclohexanepropanamine, alpha-methyl- (9CI) | HCID 15014628 | 37% |
Reaction Steps
A solution of 4.60 g 2-(3-cyclohexyl-1-methylpropyl)-1H-iso indole-1,3(2H)-dione and 7.26 g of hydrazine hydrate in 60 mL ethanol was heated to 70° C. The white precipitation was filtered off after cooling to room temperature. The mixture was washed with water and evaporated. 920 mg (37%) of a colourless oil were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148538B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-484b186c89014495931260119e3ff4b2 |
| Source note | uspto-grants-2012_04 |