HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenothiazine → 3-(Trichlorosilyl)propyl methacrylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenothiazine | HCID 7108 | — |
| Reactant | Allyl methacrylate | HCID 7274 | — |
| Reactant | Distearyl Thiodipropionate | HCID 12738 | — |
| Reactant | Trichlorosilane | HCID 24811 | — |
| Product | 3-(Trichlorosilyl)propyl methacrylate | HCID 81811 | — |
Reaction Conditions
| Temperature | 150 °C |
|---|
Reaction Steps
A methacryloxypropyl trichlorosilane was synthesized by a known method where allyl methacrylate and trichlorosilane were used as starting materials. 20 g of the obtained product and 5 mg of a styrenated phenothiazine (ANTAGE STDP-N, molecular weight was 407.6; the product of Kawaguchi Chemical Company, Ltd.) was sealed in a bottle with a threaded cap and heated in a 150° C. oil bath. The obtained product was not gelled and maintained flowability even 20 hours after the above-described treatment.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148565B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-b66a1b0f1b0f49518ee074ea3026aa38 |
| Source note | uspto-grants-2012_04 |