HRID1686371

反应详情

EQUATION

反应方程式

HRID 1686371 的结构方程式

CONDITIONS

反应条件

温度
150 °C

PROCEDURE

实验过程

A methacryloxypropyl trichlorosilane was synthesized by a known method where allyl methacrylate and trichlorosilane were used as starting materials. 20 g of the obtained product and 5 mg of a styrenated phenothiazine (ANTAGE STDP-N, molecular weight was 407.6; the product of Kawaguchi Chemical Company, Ltd.) was sealed in a bottle with a threaded cap and heated in a 150° C. oil bath. The obtained product was not gelled and maintained flowability even 20 hours after the above-described treatment.

WORKUP

后处理

  1. custom) was sealed in a bottle with
  2. customa threaded cap
  3. temperaturemaintained flowability even 20 hours after the above-described treatment