HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 58785142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 4-Chloro-3-hydroxyphenylacetic acid | HCID 3017183 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58785142 | HCID 58785142 | — |
Reaction Steps
The product of step (iii) (4 g) was added to a solution of acetyl chloride (10 ml) in ethanol (40 ml). The mixture was stirred for 1 h at RT then evaporated under reduced pressure. The residue was purified by flash column chromatography (eluent 2:1 isohexane/EtOAc) to give the subtitle compound (4.4 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148572B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-171352a18fa540cfa2f2fa0e4d8f858d |
| Source note | uspto-grants-2012_04 |