HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 55220820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,4-Difluorobenzenethiol | HCID 2778378 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 55220820 | HCID 55220820 | — |
Reaction Steps
A solution of 3,4-difluorothiophenol (3 g), ethyl iodide (1.6 ml), potassium carbonate (2.64 g) and DMF (40 ml) were charged to a flask and stirred for 2 h. The solution was partitioned between ethyl acetate and water. The organic extracts were dried (MgSO4) and evaporated under reduced pressure to give the subtitle compound (3.84 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08148572B2 |
| Source dataset | uspto-grants-2012_04 |
| ORD ID | ord-ee21a092a95d41ff9781ec7dabf02d61 |
| Source note | uspto-grants-2012_04 |